Delamination and Its Morphological Study on Hibiscus Rosa-Sinensis/Carbon Nano-Tubes/Epoxy Based-Hybrid Composites During Abrasive Water-Jet Machining Using Statistical Optimization Techniques

Document Type

Article

Publication Title

Journal of Composites Science

Abstract

The natural fiber-reinforced nanomaterial filler polymer matrix hybrid composite has superior applications in industrial and manufacturing fields due to its enhanced mechanical and machinability characteristics. However, in order to generate high-quality components, unconventional machining techniques, notably abrasive waterjet machining, have become more popular due to the inhomogeneity of composites, fiber pullout, greater surface roughness, and dimensional inaccuracy under traditional machining. Delamination typically refers to the separation that occurs along a plane parallel to the surface, such as the detachment of a coating from its underlying material or the separation between different layers within the coating itself. This paper investigates the AWJM characteristics of Hibiscus Rosa-Sinensis/Carbon nanotube/Epoxy (HRSCE)-based hybrid composite, focusing on delamination factors at entry, exit, and machining time. An L27 orthogonal array was employed to optimize process parameters, revealing that DF-entry decreased with increasing CNT (wt.%), achieving its lowest values at 3 (wt.%) CNT and 2 mm stand-off distance due to enhanced composite toughness and precise jet focus. Conversely, DF-exit increased with higher CNT (wt.%), stand-off distance and traverse speed, attributed to the composite’s increased brittleness and reduced cutting efficiency. Machining time was predominantly influenced by CNT (wt.%) (92.4%), increasing with higher reinforcement levels due to enhanced material resistance. Response surface methodology models demonstrated high accuracy in predicting machining outcomes, with errors below 3%. Contour and surface plots identified optimal conditions for minimal delamination and machining time as 3 (wt.%) CNT, low stand-off distance (2 mm), and moderate traverse speed (200 mm/min). The SEM and optimal microscopy analysis confirmed that CNT reinforcement positively influenced fiber matrix interfacial integrity and reduced surface damage.

DOI

10.3390/jcs9090509

Publication Date

9-1-2025

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