Microstructural Characterization of Novel ZrO2 Dispersion-Strengthened 9Cr Steel by Spark Plasma Sintering
Document Type
Article
Publication Title
Journal of Materials Engineering and Performance
Abstract
Technologically important Oxide Dispersion-Strengthened steels are synthesized using ZrO2 as a dispersion strengthener instead of conventionally used Y2O3. Powder metallurgical route followed by spark plasma sintering is adopted for synthesizing the material. Detailed microstructural characterization revealed a fine-grained microstructure with finer dispersoids in as-sintered and normalized condition. The stable microstructure is found to be retained even after subjecting the samples at 973 K for as long as 1000 h for long-term thermal aging trials, indicating at a possible superiority of this material over the conventional Oxide Dispersion-Strengthened steels. The yield strength is calculated by making use of microstructural parameters and predictive models, both of which shown a good agreement. Mechanical property analysis through hardness measurements was correlated with microstructural observations and compared with the conventional Oxide Dispersion-Strengthened steels. The collective results indicate ZrO2 as a potential alternate dispersoid for strengthening steel and future scope for vast exploration.
DOI
10.1007/s11665-023-08244-2
Publication Date
1-1-2023
Recommended Citation
Raghavendra, K. G.; Dasgupta, Arup; Karthiselva, N. S.; and Jayasankar, K., "Microstructural Characterization of Novel ZrO2 Dispersion-Strengthened 9Cr Steel by Spark Plasma Sintering" (2023). Open Access archive. 6199.
https://impressions.manipal.edu/open-access-archive/6199